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101.
This study reports a novel one‐step method to synthesize a new spherical support for Ziegler‐Natta catalyst under moderate condition. The support is obtained from a dispersion system where the particle stabilizer polyvinylpyrrolidone plays a main role to stabilize the spherical particles. The new chemical of the support is CH3CH2OMgOCH(CH2Cl)2, which is first reported here, has been approved by newly filed patents and also confirmed by solution NMR, solid state NMR, pyrolysis‐gas chromatography‐mass spectrometry (Py‐GC‐MS), and ICP‐MS. The support and catalyst particles have uniform distributions. The catalyst prepared from this support has been evaluated with high activity. The polypropylene obtained has high isotacticity. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2014 , 131, 41014. 相似文献
102.
Two novel iptycene-based tetramine monomers were successfully synthesized by nucleophilic aromatic substitution of triptycene-1,4-diol and pentiptycene-6,13-diol with 5-chloro-2-nitro-aniline, followed by reduction, respectively. These monomers were polymerized with 4,4-binaphthyl-1,1,8,8-tetracarboxylic dianhydride to obtain two novel iptycene-based poly[bis(benzimidazobenzisoquinolinones)]s (PBIBI–TPD and PBIBI–PPD) by a one-step, high-temperature solution polycondesation. Incorporation of iptycene groups especially the pentiptycene group in the polymer backbones improved their solubility and thermal stability. The resulting membranes exhibited good gas permeability owing to the high internal free volume elements introduced by the iptycene groups as well as high gas selectivity due to the restricted local segmental mobility arising from the interlocking of these groups in the polymer backbone. The membrane of PBIBI–PPD showed high CO2 permeability (112 barrer) and moderately good CO2/N2 and CO2/CH4 selectivity (22 and 31) for mixed gas separation. 相似文献
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Chunlei Wang Jianfen Li Juntao Yan Jianmin Sun 《Korean Journal of Chemical Engineering》2014,31(9):1547-1552
A series of hierarchical mesoporous ZSM-5 zeolites with different morphology were successfully synthesized by the CO2-in-water microemulsion method, and mesoporosity was formed without organotemplate. The different synthesis conditions, including silica alumina molar ratio, stirring time and compressed CO2 pressure, were systematically investigated to discuss the influence of these conditions on the morphology of ZSM-5 zeolite. The resulting samples were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), inductively coupled plasma (ICP) and nitrogen adsorption-desorption measurement. XRD results indicated that compressed CO2 route for the synthesis of MFI zeolites had a fast crystallization rate and good crystallinity. SEM images showed that the ZSM-5 hierarchical mesoporous ZSM-5 zeolite had a uniform chain-like crystal morphology, whereas silicalite-1 displayed a monodisperse crystal morphology. In addition, the nitrogen adsorption-desorption measurement provided sufficient evidence for the presence of hierarchical mesopores in ZSM-5 zeolite. 相似文献
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拜城县众泰煤焦化有限公司针对新疆地区冶金焦炭市场需求,对新疆地区炼焦煤资源综合利用的问题进行立项研究,丰富和完善公司产品配方库,抢占市场机遇,取得了显著的经济效益。 相似文献
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福建省鸿山热电有限公司DN3 200特大直径无顶压逆流再生离子交换器,再生成功率低,酸碱比耗大,严重影响了电厂对外供热。为此,福建省鸿山热电有限公司与西安热工院合作,进行了该设备的技改试验研究。结果表明,采用气顶压再生工艺,并采用大阻力中排,是确保大型逆流再生离子交换器再生效果的基本因素。 相似文献